X-ray Powder Diffractometer

• Fachliche Zuordnung: Chemische Festkörper- und Oberflächenforschung
• Förderung: Förderung in 2014
• Projektkennung: Deutsche Forschungsgemeinschaft (DFG) - Projektnummer 251870292

• Erstellungsjahr: 2017

Zusammenfassung der Projektergebnisse

Powder XRD measurements have been carried out on various nanomaterials synthesized in the group of Prof. Pinna in the last 3 years. Below, please find the list of publications in which XRD measurements have been used to elucidate the structure, crystallite size, etc. on the nanomaterials. In addition the diffractometer has been modified in order to carry out in situ measurements during Li/Na insertion extractions.

Projektbezogene Publikationen (Auswahl)

• (2018) Reversible Sodium and Lithium Insertion in Iron Fluoride Perovskites. Adv. Funct. Mater. (Advanced Functional Materials) 28 (29) 1802057
  Martin, Andréa; Doublet, Marie-Liesse; Kemnitz, Erhard; Pinna, Nicola
  (Siehe online unter https://doi.org/10.1002/adfm.201802057)
• Stabilization of Titanium Dioxide Nanoparticles at the Surface of Carbon Nanomaterials Promoted by Microwave Heating. Chem. Eur. J. 2015, 21 (42), 14901-14910
  R. Zhang, S. Santangelo, E. Fazio, F. Neri, M. D'Arienzo, F. Morazzoni, Y. Zhang, N. Pinna, P. A. Russo
  (Siehe online unter https://doi.org/10.1002/chem.201502433)
• Coating of Vertically Aligned Carbon Nanotubes by a Novel Manganese Oxide Atomic Layer Deposition Process for Binder-Free Hybrid Capacitors. Adv. Mater. Interfaces 2016, 3 (21), 1600313
  R. M. Silva, G. Clavel, Y. Fan, P. Amsalem, N. Koch, R. F. Silva and N. Pinna
  (Siehe online unter https://doi.org/10.1002/admi.201600313)
• Electrochemical Water Oxidation of Ultra-thin Cobalt Oxide-Based Catalyst Supported onto Aligned ZnO Nanorods. ACS Appl. Mater. Interfaces, 2016, 8 (5), 3226-3232
  N. K. Reddy, S. Winkler, N. Koch, and N. Pinna
  (Siehe online unter https://doi.org/10.1021/acsami.5b10858)
• Operando Mössbauer Spectroscopy Investigation of the Electrochemical Reaction with Lithium in Bronze-type FeF3·0.33H2O. J. Phys. Chem. C, 2016, 120 (42), pp 23933-23943
  D. E. Conte, L. Di Carlo, M. T. Sougrati, B. Fraisse, L. Stievano and N. Pinna
  (Siehe online unter https://doi.org/10.1021/acs.jpcc.6b06711)
• Hybrid Organic–Inorganic Transition-Metal Phosphonates as Precursors for Water Oxidation Electrocatalysts. Adv. Funct. Mater., 2017, 27, 1703158
  R. Zhang, P. A. Russo, A. G. Buzanich, T. Jeon, N. Pinna
  (Siehe online unter https://doi.org/10.1002/adfm.201703158)
• Phonons in Hybrid Lamellar Supercrystals. J. Phys. Chem. C, 2017, 121(3), 1990-1996
  L. Saviot, G. Caputo, N. Pinna
  (Siehe online unter https://doi.org/10.1021/acs.jpcc.6b11574)
• Synthesis of Nickel Phosphide Electrocatalysts from Hybrid Metal Phosphonates. ACS Appl. Mater. Interfaces, 2017, 9 (16), 14013–14022
  R. Zhang, P. A. Russo, M. Feist, P. Amsalem, N. Koch and N. Pinna
  (Siehe online unter https://doi.org/10.1021/acsami.7b01178)
• Cobalt-Assisted Morphology and Assembly Control of Co-Doped ZnO Nanoparticles. Nanomaterials, 2018, 8(4), 249
  X. Han, S. Wahl, P. A. Russo, N. Pinna
  (Siehe online unter https://doi.org/10.3390/nano8040249)
• Novel Synthesis of Anhydrous and Hydroxylated CuF2 Nanoparticles and Their Potential for Lithium Ion Batteries. Chem. Eur. J.
  T. Krahl, F. M. Winkelmann, A. Martin, N. Pinna, E. Kemnitz
  (Siehe online unter https://doi.org/10.1002/chem.201800207)